Information card for entry 7131539

Structure parameters

• Formula: C138 H276 Co8 F20 N14 Na8 Si28
• Calculated formula: C138 H276 Co8 F20 N14 Na8 Si28
• Title of publication: Applying Na/Co(II) bimetallic partnerships to promote multiple Co-H exchanges in polyfluoroarenes.
• Authors of publication: Logallo, Alessandra; Hevia, Eva
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 36
• Pages of publication: 5383 - 5386
• a: 21.6543 ± 0.0002 Å
• b: 17.95986 ± 0.00012 Å
• c: 27.5932 ± 0.0003 Å
• α: 90°
• β: 97.4528 ± 0.001°
• γ: 90°
• Cell volume: 10640.6 ± 0.17 ų
• Cell temperature: 173.01 ± 0.1 K
• Ambient diffraction temperature: 173.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0873
• Residual factor for significantly intense reflections: 0.0539
• Weighted residual factors for significantly intense reflections: 0.1261
• Weighted residual factors for all reflections included in the refinement: 0.1484
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No