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Information card for entry 7131561
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Coordinates | 7131561.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H23 N3 O2 |
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Calculated formula | C21 H23 N3 O2 |
Title of publication | Synthesis of 2-substituted bicyclo[1.1.0]butanes <i>via</i> zincocyclopropanation using bromoform as the carbenoid precursor. |
Authors of publication | Thai-Savard, Léa; Charette, André B |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 35 |
Pages of publication | 5273 - 5276 |
a | 15.3404 ± 0.0006 Å |
b | 5.5177 ± 0.0002 Å |
c | 21.3195 ± 0.0008 Å |
α | 90° |
β | 97.548 ± 0.002° |
γ | 90° |
Cell volume | 1788.93 ± 0.12 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0551 |
Residual factor for significantly intense reflections | 0.0379 |
Weighted residual factors for significantly intense reflections | 0.0936 |
Weighted residual factors for all reflections included in the refinement | 0.1021 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.054 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.34139 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7131561.html
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structural data.