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Information card for entry 7131569
Preview
Coordinates | 7131569.cif |
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Original paper (by DOI) | HTML |
Formula | C34 H22 Cl N O2 |
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Calculated formula | C34 H22 Cl N O2 |
Title of publication | Synthesis of indene-fused spiro-dibenz(ox)azepines <i>via</i> Rh(III)-catalyzed cascade regioselective C-H activation/annulation. |
Authors of publication | Naskar, Koushik; Karmakar, Sudip; Mondal, Imtiaj; Sarkar, Writhabrata; Roy, Shantonu; Roy, Anupam; Deb, Indubhusan |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 50 |
Pages of publication | 7751 - 7754 |
a | 8.8279 ± 0.0009 Å |
b | 11.8609 ± 0.0012 Å |
c | 13.5405 ± 0.0013 Å |
α | 68.435 ± 0.004° |
β | 73.562 ± 0.003° |
γ | 72.877 ± 0.004° |
Cell volume | 1235.5 ± 0.2 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0661 |
Residual factor for significantly intense reflections | 0.0578 |
Weighted residual factors for significantly intense reflections | 0.2117 |
Weighted residual factors for all reflections included in the refinement | 0.2241 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7131569.html
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