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Information card for entry 7131578
Preview
Coordinates | 7131578.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C40 H25 B Cl2 F15 N2 P |
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Calculated formula | C40 H25 B Cl2 F15 N2 P |
Title of publication | Reactivity of frustrated Lewis pairs with BOC protected diazocarboxylates: FLP capture of diazene. |
Authors of publication | Hussain, Zahid; Luo, Yong-An; Wu, Yile; Qu, Zheng-Wang; Grimme, Stefan; Stephan, Douglas W. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 41 |
Pages of publication | 6191 - 6194 |
a | 11.195 ± 0.0003 Å |
b | 18.3322 ± 0.0004 Å |
c | 19.4142 ± 0.0005 Å |
α | 90° |
β | 105.076 ± 0.001° |
γ | 90° |
Cell volume | 3847.22 ± 0.17 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0502 |
Residual factor for significantly intense reflections | 0.048 |
Weighted residual factors for significantly intense reflections | 0.1361 |
Weighted residual factors for all reflections included in the refinement | 0.138 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7131578.html
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