Crystallography Open Database

Information card for entry 7131604

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Coordinates	7131604.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Hexa-((bis-trimethylsilyl)methyl)-hexa-stannane
Formula	C42 H114 Si12 Sn6
Calculated formula	C42 H114 Si12 Sn6
Title of publication	Disproportionation of Sn(II){CH(SiMe<sub>3</sub>)<sub>2</sub>}<sub>2</sub> to ˙Sn(III){CH(SiMe<sub>3</sub>)<sub>2</sub>}<sub>3</sub> and ˙Sn(I){CH(SiMe<sub>3</sub>)<sub>2</sub>}: characterization of the Sn(I) product.
Authors of publication	Mears, Kristian L.; Ruiz, Bronson; Nguyen, Gia-Ann; Zou, Wenxing; Fettinger, James C.; Power, Philip P.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2023
Journal volume	59
Journal issue	42
Pages of publication	6399 - 6402
a	13.2745 ± 0.0004 Å
b	13.7262 ± 0.0003 Å
c	22.639 ± 0.0006 Å
α	86.4949 ± 0.0014°
β	76.8746 ± 0.0014°
γ	72.0005 ± 0.0013°
Cell volume	3820.46 ± 0.18 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0411
Residual factor for significantly intense reflections	0.0314
Weighted residual factors for significantly intense reflections	0.0697
Weighted residual factors for all reflections included in the refinement	0.0739
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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