Information card for entry 7131746

Structure parameters

• Formula: C32 H48 N4 O14
• Calculated formula: C32 H48 N4 O14
• Title of publication: Catalytic asymmetric interrupted Attanasi reaction: access to fused 2,3-dihydropyrroles with vicinal quaternary carbons.
• Authors of publication: Chen, Yun-Xuan; Han, Tian-Jiao; Xiao, Xiao; Wang, Min-Can; Mei, Guang-Jian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 52
• Pages of publication: 8103 - 8106
• a: 9.4928 ± 0.0009 Å
• b: 9.8026 ± 0.0009 Å
• c: 11.3802 ± 0.0008 Å
• α: 102.528 ± 0.007°
• β: 110.036 ± 0.008°
• γ: 102.007 ± 0.008°
• Cell volume: 924.02 ± 0.16 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.075
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1335
• Weighted residual factors for all reflections included in the refinement: 0.1674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No