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Information card for entry 7131855
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Coordinates | 7131855.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | ORGANIC |
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Chemical name | spiro-indolocyclopentene |
Formula | C38 H32 Br2 N2 S2 |
Calculated formula | C38 H32 Br2 N2 S2 |
Title of publication | Base-mediated cascade synthesis of indole diolefins: a route to spiro[cyclopentene-indole]thiones and thiepino[2,3-<i>b</i>]indoles. |
Authors of publication | Muthusamy, Sengodagounder; Naveen, Ramasamy; Kumar, Muniyappankovilthottam Devaraj Senthil |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 55 |
Pages of publication | 8560 - 8563 |
a | 9.382 ± 0.002 Å |
b | 10.472 ± 0.002 Å |
c | 17.945 ± 0.004 Å |
α | 88.563 ± 0.006° |
β | 78.673 ± 0.006° |
γ | 72.965 ± 0.006° |
Cell volume | 1651.9 ± 0.6 Å3 |
Cell temperature | 303 ± 2 K |
Ambient diffraction temperature | 303 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.2098 |
Residual factor for significantly intense reflections | 0.0637 |
Weighted residual factors for significantly intense reflections | 0.1534 |
Weighted residual factors for all reflections included in the refinement | 0.2212 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.931 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | Mokα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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