Information card for entry 7131894

Structure parameters

• Formula: C60 H84 Cl3 N6 P3 Pd Si3
• Calculated formula: C60 H84 Cl3 N6 P3 Pd Si3
• Title of publication: Synthesis of a homoleptic tris(silylene)-palladium(0) complex and a silylyne-bridged tetranuclear palladium cluster
• Authors of publication: Sekiguchi, Jueri; Kazama, Yugo; Ishii, Akihiko; Nakata, Norio
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 15.16 ± 0.003 Å
• b: 15.382 ± 0.003 Å
• c: 15.98 ± 0.003 Å
• α: 108.61 ± 0.003°
• β: 104.396 ± 0.003°
• γ: 100.007 ± 0.003°
• Cell volume: 3288.1 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1171
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for significantly intense reflections: 0.1314
• Weighted residual factors for all reflections included in the refinement: 0.1495
• Goodness-of-fit parameter for all reflections included in the refinement: 0.829
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No