Information card for entry 7131937

Structure parameters

• Formula: C52 H58 Al F36 I O6 P4 Sb Ta
• Calculated formula: C52 H56 Al F36 I O6 P4 Sb Ta
• Title of publication: Ring Expansion vs. Addition – Reactivity of a cyclo-P4 Complex Towards Pnictogenium Cations
• Authors of publication: Riesinger, Christoph; Erhard, Alexander; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 10.6596 ± 0.0004 Å
• b: 16.9425 ± 0.0005 Å
• c: 21.4058 ± 0.0007 Å
• α: 109.867 ± 0.003°
• β: 91.228 ± 0.003°
• γ: 98.222 ± 0.003°
• Cell volume: 3588.2 ± 0.2 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.129
• Weighted residual factors for all reflections included in the refinement: 0.1427
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No