Information card for entry 7131940

Structure parameters

• Formula: C57 H64 Al F36 O7 P9 Ta2
• Calculated formula: C57 H64 Al F36 O7 P9 Ta2
• Title of publication: Ring Expansion vs. Addition – Reactivity of a cyclo-P4 Complex Towards Pnictogenium Cations
• Authors of publication: Riesinger, Christoph; Erhard, Alexander; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 15.59941 ± 0.00008 Å
• b: 16.56789 ± 0.00007 Å
• c: 16.9 ± 0.00007 Å
• α: 112.531 ± 0.0004°
• β: 99.2052 ± 0.0004°
• γ: 91.6604 ± 0.0004°
• Cell volume: 3962.9 ± 0.03 ų
• Cell temperature: 123.01 ± 0.1 K
• Ambient diffraction temperature: 123.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.025
• Residual factor for significantly intense reflections: 0.0249
• Weighted residual factors for significantly intense reflections: 0.0628
• Weighted residual factors for all reflections included in the refinement: 0.0628
• Goodness-of-fit parameter for all reflections included in the refinement: 1.149
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No