In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes
Authors of publication
Goodall, Joe C.; Sajjad, Muhammad Arif; Thompson, Emily A.; Page, Samuel J.; Kerrigan, Adam M.; Jenkins, Huw T.; Lynam, Jason Martin; Macgregor, Stuart Alan; Weller, Andrew S.
Journal of publication
Chemical Communications
Year of publication
2023
a
24.3315 ± 0.0002 Å
b
10.2609 ± 0.0001 Å
c
11.2141 ± 0.0001 Å
α
90°
β
90°
γ
90°
Cell volume
2799.75 ± 0.04 Å3
Cell temperature
110.05 ± 0.1 K
Ambient diffraction temperature
110.05 ± 0.1 K
Number of distinct elements
7
Space group number
33
Hermann-Mauguin space group symbol
P n a 21
Hall space group symbol
P 2c -2n
Residual factor for all reflections
0.0232
Residual factor for significantly intense reflections
0.0227
Weighted residual factors for significantly intense reflections
0.0595
Weighted residual factors for all reflections included in the refinement
0.0598
Goodness-of-fit parameter for all reflections included in the refinement
