Information card for entry 7132028

Structure parameters

• Formula: C65 H60 B F15 N2 O P Sn
• Calculated formula: C65 H60 B F15 N2 O P Sn
• Title of publication: Stannyl phosphaketene as a synthon for phosphorus analogues of β-lactam
• Authors of publication: Luo, Yong-An; Zhao, Zhao; Chen, Ting; Li, Yanguo; Zhao, Yufen; Stephan, Douglas W.; Wu, Yile
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 15.5036 ± 0.0007 Å
• b: 25.6431 ± 0.0012 Å
• c: 15.6976 ± 0.0007 Å
• α: 90°
• β: 91.655 ± 0.002°
• γ: 90°
• Cell volume: 6238.1 ± 0.5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0809
• Weighted residual factors for all reflections included in the refinement: 0.0816
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No