Information card for entry 7132083

Structure parameters

• Formula: C26 H21 F Ge
• Calculated formula: C26 H21 F Ge
• Title of publication: Highly selective α-hydrogermylation of alkynes catalyzed by an in-situ generated bulky NHC–cobalt complex
• Authors of publication: Bołt, Małgorzata; Mermela, Aleksandra; Żak, Patrycja
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 10.1158 ± 0.0003 Å
• b: 10.3844 ± 0.0003 Å
• c: 19.5215 ± 0.0005 Å
• α: 90°
• β: 94.317 ± 0.002°
• γ: 90°
• Cell volume: 2044.85 ± 0.1 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0633
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No