Information card for entry 7132109

Structure parameters

• Formula: C16 H45 Fe N5 Si4
• Calculated formula: C16 H45 Fe N5 Si4
• Title of publication: A low-coordinate iron organoazide complex.
• Authors of publication: Gonzalez, Andres; Demeshko, Serhiy; Meyer, Franc; Werncke, C. Gunnar
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• a: 8.7622 ± 0.0002 Å
• b: 16.0342 ± 0.0007 Å
• c: 20.4887 ± 0.0007 Å
• α: 90°
• β: 101.245 ± 0.001°
• γ: 90°
• Cell volume: 2823.3 ± 0.17 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0798
• Weighted residual factors for all reflections included in the refinement: 0.0835
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No