Information card for entry 7132112

Structure parameters

• Formula: C16 H45 Fe N4.31 Si4
• Calculated formula: C16 H45 Fe N4.308 Si4
• Title of publication: A low-coordinate iron organoazide complex.
• Authors of publication: Gonzalez, Andres; Demeshko, Serhiy; Meyer, Franc; Werncke, C. Gunnar
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• a: 8.8341 ± 0.0017 Å
• b: 15.935 ± 0.003 Å
• c: 20.441 ± 0.004 Å
• α: 90°
• β: 100.299 ± 0.006°
• γ: 90°
• Cell volume: 2831.1 ± 0.9 ų
• Cell temperature: 80 K
• Ambient diffraction temperature: 80 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1301
• Residual factor for significantly intense reflections: 0.0821
• Weighted residual factors for significantly intense reflections: 0.2032
• Weighted residual factors for all reflections included in the refinement: 0.2175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No