Information card for entry 7132174

Structure parameters

• Formula: C30 H41 N O5 S Si
• Calculated formula: C30 H41 N O5 S Si
• SMILES: S(=O)(=O)(N([C@@H]1O[C@H](CO[Si](C(C)C)(C(C)C)C(C)C)[C@H](O)C=C1)c1c(C#Cc2ccccc2)cccc1)C
• Title of publication: Facile and Stereospecific Synthesis of Diverse β-N-Glycosyl Sulfonamide Scaffolds via Palladium Catalysis
• Authors of publication: Zhong, Lei; Wang, Qunliang; Wang, Yujuan; Cheng, Yiyang; Xiong, Yimeng; Peng, Haibo; Zhou, Zhen; He, Yun; Dai, Yuanwei
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 7.5387 ± 0.0003 Å
• b: 13.4947 ± 0.0006 Å
• c: 30.0141 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3053.4 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0799
• Residual factor for significantly intense reflections: 0.0515
• Weighted residual factors for significantly intense reflections: 0.109
• Weighted residual factors for all reflections included in the refinement: 0.1242
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No