Information card for entry 7132316
| Formula |
C72 H60 F12 N8 O8 |
| Calculated formula |
C72 H60 F12 N8 O8 |
| Title of publication |
The Cyclization/Rearrangement of α-Hydroxy Ketones with Trifluoromethyl N-acylhydrazones to Synthesize Multi-substituted Trifluoromethyloxazolines |
| Authors of publication |
Wang, Junjiao; Shang, Yongwei; Zhao, Xiujuan; Cui, Zhenli; Li, Yang; Wang, Ke-Hu; Huang, Danfeng; Hu, Yulai; Wang, Na; Feng, Lei |
| Journal of publication |
Chemical Communications |
| Year of publication |
2023 |
| a |
14.6254 ± 0.0002 Å |
| b |
14.0014 ± 0.0002 Å |
| c |
33.2503 ± 0.0004 Å |
| α |
90° |
| β |
97.31 ± 0.001° |
| γ |
90° |
| Cell volume |
6753.53 ± 0.16 Å3 |
| Cell temperature |
300.51 ± 0.1 K |
| Ambient diffraction temperature |
300.51 ± 0.1 K |
| Number of distinct elements |
5 |
| Space group number |
9 |
| Hermann-Mauguin space group symbol |
C 1 c 1 |
| Hall space group symbol |
C -2yc |
| Residual factor for all reflections |
0.0467 |
| Residual factor for significantly intense reflections |
0.0437 |
| Weighted residual factors for significantly intense reflections |
0.1181 |
| Weighted residual factors for all reflections included in the refinement |
0.1213 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.031 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7132316.html
