Crystallography Open Database

Information card for entry 7132334

Preview

Coordinates	7132334.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H22 N2
Calculated formula	C24 H22 N2
Title of publication	Synthesis of 3-Aminotetrahydro-1H-carbazols by Visible-Light Photocatalyzed Cycloaddition of Cyclopropylanilines with 2-Alkenylarylisocyanides
Authors of publication	Zhang, Xiaofei; Wang, Yao; Liu, Jiaxin; Tian, Chengpeng; Li, Xiang; Xie, Pan; Zhu, Zhen-Yu; Yao, Tuanli
Journal of publication	Chemical Communications
Year of publication	2023
a	9.4607 ± 0.0007 Å
b	10.9217 ± 0.0008 Å
c	17.9906 ± 0.0014 Å
α	90°
β	96.556 ± 0.002°
γ	90°
Cell volume	1846.8 ± 0.2 Å³
Cell temperature	276 ± 2 K
Ambient diffraction temperature	276 ± 2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.122
Residual factor for significantly intense reflections	0.0419
Weighted residual factors for significantly intense reflections	0.0816
Weighted residual factors for all reflections included in the refinement	0.0978
Goodness-of-fit parameter for all reflections included in the refinement	0.828
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7132334.html