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Information card for entry 7132369
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Coordinates | 7132369.cif |
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Original paper (by DOI) | HTML |
Formula | C17 H26 O5 Si |
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Calculated formula | C17 H26 O5 Si |
Title of publication | Total synthesis of highly oxygenated phomopsol B <i>via</i> acid-induced etherification to construct a bridged structure. |
Authors of publication | Kawamoto, Yuichiro; Nishitani, Ayaka; Yoshimura, Yukari; Kobayashi, Toyoharu; Ito, Hisanaka |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 60 |
Journal issue | 1 |
Pages of publication | 95 - 97 |
a | 7.9252 ± 0.0008 Å |
b | 9.8381 ± 0.0009 Å |
c | 12.6943 ± 0.0012 Å |
α | 98.475 ± 0.001° |
β | 107.944 ± 0.001° |
γ | 106.441 ± 0.001° |
Cell volume | 872.76 ± 0.15 Å3 |
Cell temperature | 90 K |
Ambient diffraction temperature | 90 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0402 |
Residual factor for significantly intense reflections | 0.0369 |
Weighted residual factors for significantly intense reflections | 0.0974 |
Weighted residual factors for all reflections included in the refinement | 0.0998 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Diffraction radiation X-ray symbol | K-L~3~ |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7132369.html
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Users of the data should acknowledge the original authors of the
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