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Information card for entry 7132404
Preview
Coordinates | 7132404.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H35 N O4 S2 |
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Calculated formula | C41 H35 N O4 S2 |
Title of publication | Cascade radical cyclization on 3-propargyl-2-alkenyl indole gives stereoselective access to cyclohepta[<i>b</i>]indole over carbazole. |
Authors of publication | Gharpure, Santosh J.; Kumari, Sanyog |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 5 |
Pages of publication | 538 - 541 |
a | 19.4285 ± 0.0018 Å |
b | 11.6342 ± 0.0008 Å |
c | 16.4121 ± 0.0014 Å |
α | 90° |
β | 113.21 ± 0.01° |
γ | 90° |
Cell volume | 3409.5 ± 0.6 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1321 |
Residual factor for significantly intense reflections | 0.0748 |
Weighted residual factors for significantly intense reflections | 0.1893 |
Weighted residual factors for all reflections included in the refinement | 0.2547 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.968 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7132404.html
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