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Information card for entry 7132444
Preview
Coordinates | 7132444.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H18 N2 O |
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Calculated formula | C24 H18 N2 O |
Title of publication | Pd/Brønsted acid catalysed intramolecular <i>N</i>-allylation of indoles and pyrroles with alkynes for the synthesis of N-fused heterocycles. |
Authors of publication | Bhoi, Saswat Ranjan; Debnath, Chhanda; Gandhi, Shikha |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 4 |
Pages of publication | 428 - 431 |
a | 6.3722 ± 0.0005 Å |
b | 13.4572 ± 0.0011 Å |
c | 14.9777 ± 0.0014 Å |
α | 66.406 ± 0.008° |
β | 89.765 ± 0.007° |
γ | 84.766 ± 0.006° |
Cell volume | 1171.35 ± 0.19 Å3 |
Cell temperature | 101 ± 1 K |
Ambient diffraction temperature | 101 ± 1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0617 |
Residual factor for significantly intense reflections | 0.0492 |
Weighted residual factors for significantly intense reflections | 0.1481 |
Weighted residual factors for all reflections included in the refinement | 0.1556 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7132444.html
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