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Information card for entry 7132460
Preview
Coordinates | 7132460.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H22 O6 |
---|---|
Calculated formula | C22 H22 O6 |
Title of publication | Intramolecular Ni-catalyzed reductive coupling enables enantiodivergent synthesis of linoxepin. |
Authors of publication | Liu, Zi-Hao; Xiao, Jian; Zhai, Qian-Qian; Tang, Xi; Xu, Li-Jun; Zhuang, Zhi-Yuan; Wang, Ya-Wen; Peng, Yu |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 6 |
Pages of publication | 694 - 697 |
a | 8.41567 ± 0.00015 Å |
b | 11.8302 ± 0.0003 Å |
c | 18.4063 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1832.51 ± 0.06 Å3 |
Cell temperature | 149.99 ± 0.1 K |
Ambient diffraction temperature | 149.99 ± 0.1 K |
Number of distinct elements | 3 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.037 |
Residual factor for significantly intense reflections | 0.0339 |
Weighted residual factors for significantly intense reflections | 0.085 |
Weighted residual factors for all reflections included in the refinement | 0.087 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7132460.html
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structural data.