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Information card for entry 7132491
Preview
Coordinates | 7132491.cif |
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Original paper (by DOI) | HTML |
Formula | C55.2 H57 B F0.2 N4 Ni2 O4 |
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Calculated formula | C54 H56 B N4 Ni2 O4 |
Title of publication | Contrasting reactivity of B-Cl and B-H bonds at [Ni(IMes)<sub>2</sub>] to form unsupported Ni-boryls. |
Authors of publication | Audsley, Gabrielle; Carpentier, Ambre; Pécharman, Anne-Frédérique; Wright, James; Roseveare, Thomas M.; Clark, Ewan R.; Macgregor, Stuart A.; Riddlestone, Ian M. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 7 |
Pages of publication | 874 - 877 |
a | 12.0673 ± 0.0003 Å |
b | 13.458 ± 0.0005 Å |
c | 15.2235 ± 0.0005 Å |
α | 91.823 ± 0.003° |
β | 99.146 ± 0.003° |
γ | 97.973 ± 0.003° |
Cell volume | 2413.63 ± 0.14 Å3 |
Cell temperature | 150.01 ± 0.1 K |
Ambient diffraction temperature | 150.01 ± 0.1 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.057 |
Residual factor for significantly intense reflections | 0.0426 |
Weighted residual factors for significantly intense reflections | 0.1024 |
Weighted residual factors for all reflections included in the refinement | 0.1108 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.015 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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