Information card for entry 7132495

Structure parameters

• Formula: C109 H138 Au2 B4 Br2 N10
• Calculated formula: C109 H138 Au2 B4 Br2 N10
• Title of publication: Stepwise and selective synthesis of chelating, multimetallic and mixed-metal π-diborene complexes.
• Authors of publication: Duwe, Dario; Saha, Koushik; Endres, Lukas; Brückner, Tobias; Dewhurst, Rian D.; Dietz, Maximilian; Radacki, Krzysztof; Fantuzzi, Felipe; Braunschweig, Holger
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 9
• Pages of publication: 1120 - 1123
• a: 12.547 ± 0.006 Å
• b: 18.489 ± 0.008 Å
• c: 21.362 ± 0.008 Å
• α: 90°
• β: 93.295 ± 0.013°
• γ: 90°
• Cell volume: 4947 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0516
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0697
• Weighted residual factors for all reflections included in the refinement: 0.0753
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~2,3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No