Information card for entry 7132501

Structure parameters

• Formula: C51 H65 B2 Cl4 Cu4 N5
• Calculated formula: C51 H65 B2 Cl4 Cu4 N5
• Title of publication: Stepwise and selective synthesis of chelating, multimetallic and mixed-metal π-diborene complexes.
• Authors of publication: Duwe, Dario; Saha, Koushik; Endres, Lukas; Brückner, Tobias; Dewhurst, Rian D.; Dietz, Maximilian; Radacki, Krzysztof; Fantuzzi, Felipe; Braunschweig, Holger
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 9
• Pages of publication: 1120 - 1123
• a: 15.0923 ± 0.0011 Å
• b: 17.1901 ± 0.0014 Å
• c: 25.434 ± 0.002 Å
• α: 102.384 ± 0.003°
• β: 91.28 ± 0.002°
• γ: 90.589 ± 0.003°
• Cell volume: 6442.6 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1342
• Residual factor for significantly intense reflections: 0.094
• Weighted residual factors for significantly intense reflections: 0.249
• Weighted residual factors for all reflections included in the refinement: 0.2747
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No