Information card for entry 7132518

Structure parameters

• Formula: C130 H162 K2 Mg2 N4 O4
• Calculated formula: C130 H162 K2 Mg2 N4 O4
• Title of publication: Steric control of Mg-Mg bond formation <i>vs.</i> N₂ activation in the reduction of bulky magnesium diamide complexes.
• Authors of publication: Mondal, Rahul; Evans, Matthew J.; Nguyen, Dat T.; Rajeshkumar, Thayalan; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1016 - 1019
• a: 58.863 ± 0.002 Å
• b: 9.9267 ± 0.0001 Å
• c: 34.1523 ± 0.0012 Å
• α: 90°
• β: 144.652 ± 0.008°
• γ: 90°
• Cell volume: 11545 ± 2 ų
• Cell temperature: 123.01 ± 0.1 K
• Ambient diffraction temperature: 123.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.1127
• Weighted residual factors for all reflections included in the refinement: 0.1165
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No