Information card for entry 7132520

Structure parameters

• Formula: C118 H178 K2 Mg2 N4 O4
• Calculated formula: C118 H178 K2 Mg2 N4 O4
• Title of publication: Steric control of Mg-Mg bond formation <i>vs.</i> N₂ activation in the reduction of bulky magnesium diamide complexes.
• Authors of publication: Mondal, Rahul; Evans, Matthew J.; Nguyen, Dat T.; Rajeshkumar, Thayalan; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1016 - 1019
• a: 19.617 ± 0.004 Å
• b: 21.324 ± 0.004 Å
• c: 25.718 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10758 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0736
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1807
• Weighted residual factors for all reflections included in the refinement: 0.1901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.7109 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No