Crystallography Open Database

Information card for entry 7132536

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Coordinates	7132536.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H51 Cl4 Ga N2 O2 P2
Calculated formula	C40 H41 Cl4 Ga N2 O P2
Title of publication	Addition and NN bond cleavage of diazo-compounds by phosphino-phosphenium cations.
Authors of publication	Kim, Hyehwang; Lough, Alan; Qu, Zheng-Wang; Grimme, Stefan; Stephan, Douglas W.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	8
Pages of publication	1031 - 1034
a	11.2788 ± 0.001 Å
b	13.1565 ± 0.0012 Å
c	16.1265 ± 0.0015 Å
α	95.445 ± 0.006°
β	108.409 ± 0.005°
γ	91.577 ± 0.006°
Cell volume	2256.1 ± 0.4 Å³
Cell temperature	149.98 K
Ambient diffraction temperature	149.98 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1215
Residual factor for significantly intense reflections	0.0787
Weighted residual factors for significantly intense reflections	0.185
Weighted residual factors for all reflections included in the refinement	0.2169
Goodness-of-fit parameter for all reflections included in the refinement	1.0831
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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