Information card for entry 7132538

Structure parameters

• Formula: C43 H33.5 Cl4 F2 Ga N3 P2
• Calculated formula: C43 H33.5 Cl4 F2 Ga N3 P2
• Title of publication: Addition and NN bond cleavage of diazo-compounds by phosphino-phosphenium cations.
• Authors of publication: Kim, Hyehwang; Lough, Alan; Qu, Zheng-Wang; Grimme, Stefan; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1031 - 1034
• a: 12.1657 ± 0.0009 Å
• b: 18.5693 ± 0.0011 Å
• c: 19.1345 ± 0.0013 Å
• α: 90°
• β: 102.701 ± 0.005°
• γ: 90°
• Cell volume: 4216.9 ± 0.5 ų
• Cell temperature: 150.02 K
• Ambient diffraction temperature: 150.02 K
• Number of distinct elements: 7
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.1302
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for significantly intense reflections: 0.1489
• Weighted residual factors for all reflections included in the refinement: 0.1843
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0654
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No