Crystallography Open Database

Information card for entry 7132609

Preview

Coordinates	7132609.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H43 Cl O P2 Pd
Calculated formula	C48 H43 Cl O P2 Pd
Title of publication	Palladium-catalyzed allylation and carbonylation: access to allylhydrazones and allyl acylhydrazones.
Authors of publication	Liang, Qianqian; Cai, Yan; Jiang, Wenjun; Pang, Mengdi; Fan, Liming; Zhang, Guoying
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	12
Pages of publication	1638 - 1641
a	19.3124 ± 0.0017 Å
b	18.4281 ± 0.0016 Å
c	12.7741 ± 0.0011 Å
α	90°
β	103.027 ± 0.003°
γ	90°
Cell volume	4429.2 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.1566
Residual factor for significantly intense reflections	0.0929
Weighted residual factors for significantly intense reflections	0.2139
Weighted residual factors for all reflections included in the refinement	0.2385
Goodness-of-fit parameter for all reflections included in the refinement	1.105
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7132609.html