Crystallography Open Database

Information card for entry 7132614

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Coordinates	7132614.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H33 O3 P
Calculated formula	C30 H33 O3 P
Title of publication	CAMDOL-enabled diastereoselective synthesis of α-substituted phosphonates.
Authors of publication	Huang, Yu; Zhang, Yulong; Pan, Li; Wu, Qian; Li, Ning; Shi, Enxue; Xiao, Junhua
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	14
Pages of publication	1924 - 1927
a	10.97433 ± 0.00016 Å
b	9.78846 ± 0.00014 Å
c	11.7517 ± 0.0002 Å
α	90°
β	102.023 ± 0.0016°
γ	90°
Cell volume	1234.7 ± 0.03 Å³
Cell temperature	179.99 ± 0.1 K
Ambient diffraction temperature	179.99 ± 0.1 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0307
Residual factor for significantly intense reflections	0.0301
Weighted residual factors for significantly intense reflections	0.0786
Weighted residual factors for all reflections included in the refinement	0.079
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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