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Information card for entry 7132636
Preview
Coordinates | 7132636.cif |
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Original paper (by DOI) | HTML |
Formula | C54 H72 B2 N4 Si |
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Calculated formula | C54 H72 B2 N4 Si |
Title of publication | Hydrosilylation of BB triple bonds: catalyst- and reductant-free construction of B-Si bonds and B<sub>2</sub>Si heterocycles. |
Authors of publication | Brückner, Tobias; Duwe, Dario; Fantuzzi, Felipe; Heß, Merlin; Dewhurst, Rian D.; Radacki, Krzysztof; Braunschweig, Holger |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 24 |
Pages of publication | 3259 - 3262 |
a | 12.4737 ± 0.0003 Å |
b | 14.971 ± 0.0004 Å |
c | 26.1547 ± 0.0007 Å |
α | 90° |
β | 92.786 ± 0.001° |
γ | 90° |
Cell volume | 4878.5 ± 0.2 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0583 |
Residual factor for significantly intense reflections | 0.0452 |
Weighted residual factors for significantly intense reflections | 0.1079 |
Weighted residual factors for all reflections included in the refinement | 0.1175 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7132636.html
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