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Information card for entry 7132639
Preview
Coordinates | 7132639.cif |
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Original paper (by DOI) | HTML |
Formula | C54 H72 B2 N4 Si |
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Calculated formula | C54 H72 B2 N4 Si |
Title of publication | Hydrosilylation of BB triple bonds: catalyst- and reductant-free construction of B-Si bonds and B<sub>2</sub>Si heterocycles. |
Authors of publication | Brückner, Tobias; Duwe, Dario; Fantuzzi, Felipe; Heß, Merlin; Dewhurst, Rian D.; Radacki, Krzysztof; Braunschweig, Holger |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 24 |
Pages of publication | 3259 - 3262 |
a | 24.18452 ± 0.00019 Å |
b | 11.44862 ± 0.00012 Å |
c | 68.9173 ± 0.0007 Å |
α | 90° |
β | 90.4985 ± 0.0008° |
γ | 90° |
Cell volume | 19081.1 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | I 1 2/a 1 |
Hall space group symbol | -I 2ya |
Residual factor for all reflections | 0.0634 |
Residual factor for significantly intense reflections | 0.0546 |
Weighted residual factors for significantly intense reflections | 0.137 |
Weighted residual factors for all reflections included in the refinement | 0.1427 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7132639.html
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