Crystallography Open Database

Information card for entry 7132720

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Coordinates	7132720.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H96 N20 P4 U2
Calculated formula	C40 H96 N20 P4 U2
Title of publication	Temperature induced single-crystal to single-crystal transformation of uranium azide complexes.
Authors of publication	Li, Kai; Rajeshkumar, Thayalan; Zhao, Yue; Wang, Tianwei; Maron, Laurent; Zhu, Congqing
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	21
Pages of publication	2966 - 2969
a	25.24 ± 0.004 Å
b	10.392 ± 0.002 Å
c	25.465 ± 0.005 Å
α	90°
β	110.915 ± 0.006°
γ	90°
Cell volume	6239 ± 2 Å³
Cell temperature	313 K
Ambient diffraction temperature	313 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1364
Residual factor for significantly intense reflections	0.0558
Weighted residual factors for significantly intense reflections	0.098
Weighted residual factors for all reflections included in the refinement	0.1252
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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