Information card for entry 7132780

Structure parameters

• Formula: C36 H98 I2 K O11 Si8 U
• Calculated formula: C36 H98 I2 K O11 Si8 U
• Title of publication: Solution and solid-state characterization of rare silyluranium(III) complexes.
• Authors of publication: Lin, Nathan J.; Zeller, Matthias; Bart, Suzanne C.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 29
• Pages of publication: 3954 - 3957
• a: 14.8717 ± 0.0005 Å
• b: 15.8095 ± 0.0005 Å
• c: 28.9025 ± 0.0009 Å
• α: 90°
• β: 103.785 ± 0.002°
• γ: 90°
• Cell volume: 6599.7 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.1344
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.1003
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No