Information card for entry 7132889
| Formula |
C16 H21 N O2 |
| Calculated formula |
C16 H21 N O2 |
| Title of publication |
Stereocontrol in an intermolecular Schmidt reaction of equilibrating hydroxyalkyl allylic azides. |
| Authors of publication |
Liu, Ruzhang; Wang, Juan; Wu, Hao; Quan, Xianfeng; Wang, Shilin; Guo, Jiandong; Wang, Yang; Li, Heting |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2024 |
| Journal volume |
60 |
| Journal issue |
32 |
| Pages of publication |
4362 - 4365 |
| a |
21.9697 ± 0.0013 Å |
| b |
6.3504 ± 0.0003 Å |
| c |
23.532 ± 0.0013 Å |
| α |
90° |
| β |
114.886 ± 0.002° |
| γ |
90° |
| Cell volume |
2978.3 ± 0.3 Å3 |
| Cell temperature |
296.13 K |
| Ambient diffraction temperature |
296.13 K |
| Number of distinct elements |
4 |
| Space group number |
15 |
| Hermann-Mauguin space group symbol |
C 1 2/c 1 |
| Hall space group symbol |
-C 2yc |
| Residual factor for all reflections |
0.1179 |
| Residual factor for significantly intense reflections |
0.0579 |
| Weighted residual factors for significantly intense reflections |
0.1468 |
| Weighted residual factors for all reflections included in the refinement |
0.1743 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.019 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7132889.html
