Information card for entry 7132892

Structure parameters

• Formula: C24 H39 N O3
• Calculated formula: C24 H39 N O3
• Title of publication: Stereocontrol in an intermolecular Schmidt reaction of equilibrating hydroxyalkyl allylic azides.
• Authors of publication: Liu, Ruzhang; Wang, Juan; Wu, Hao; Quan, Xianfeng; Wang, Shilin; Guo, Jiandong; Wang, Yang; Li, Heting
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 32
• Pages of publication: 4362 - 4365
• a: 10.4856 ± 0.0019 Å
• b: 14.332 ± 0.002 Å
• c: 14.635 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2199.3 ± 0.6 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1041
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.0946
• Weighted residual factors for all reflections included in the refinement: 0.1096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No