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Information card for entry 7132899
Preview
Coordinates | 7132899.cif |
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Original paper (by DOI) | HTML |
Formula | C31 H37 N O3 S Si |
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Calculated formula | C31 H37 N O3 S Si |
Title of publication | Radical cascade silylation/cyclization of 1,7-dienes to access silyl-substituted benzo[<i>b</i>]azepin-2-ones. |
Authors of publication | Zhang, Zhen; Lu, Lichao; Li, Guiling; Sheng, Xiaoyu; Zhang, Yijia; Yang, Lin; Zhao, Jiaqi; Xie, Lei; Li, Jiazhu; Sun, Kai |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 31 |
Pages of publication | 4206 - 4209 |
a | 9.462 ± 0.0009 Å |
b | 9.6433 ± 0.0009 Å |
c | 17.6776 ± 0.0019 Å |
α | 75.612 ± 0.002° |
β | 75.789 ± 0.002° |
γ | 87.111 ± 0.003° |
Cell volume | 1514.5 ± 0.3 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1866 |
Residual factor for significantly intense reflections | 0.128 |
Weighted residual factors for significantly intense reflections | 0.3297 |
Weighted residual factors for all reflections included in the refinement | 0.353 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.176 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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