Information card for entry 7132920

Structure parameters

• Formula: C56 H40 As4 Br4 Cu4 Mo8 O16 Sb4
• Calculated formula: C56 H40 As4 Br4 Cu4 Mo8 O16 Sb4
• Title of publication: Supramolecular compounds assembled from the heteroleptic tetrahedral complex [{CpMo(CO)₂}₂(μ,η²-AsSb)] and metal salts.
• Authors of publication: Elsayed Moussa, Mehdi; Shelyganov, Pavel A.; Seidl, Michael; Zimmermann, Lisa; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 35
• Pages of publication: 4703 - 4706
• a: 14.9733 ± 0.0004 Å
• b: 15.0851 ± 0.0005 Å
• c: 17.339 ± 0.0005 Å
• α: 89.022 ± 0.002°
• β: 88.933 ± 0.002°
• γ: 70.588 ± 0.003°
• Cell volume: 3692.9 ± 0.2 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0561
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.0769
• Weighted residual factors for all reflections included in the refinement: 0.0801
• Goodness-of-fit parameter for all reflections included in the refinement: 1.247
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No