Information card for entry 7132926

Structure parameters

• Formula: C32 H36 Si4
• Calculated formula: C32 H36 Si4
• Title of publication: Angle-strained sila-cycloalkynes.
• Authors of publication: Wakefield, 4th, Herbert; Melvin, Sophia J.; Jiang, Jennifer; Kevlishvili, Ilia; Siegler, Maxime A.; Craig, Stephen L.; Kulik, Heather J.; Klausen, Rebekka S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 36
• Pages of publication: 4842 - 4845
• a: 24.3501 ± 0.0013 Å
• b: 11.0409 ± 0.0004 Å
• c: 25.4353 ± 0.0011 Å
• α: 90°
• β: 115.708 ± 0.006°
• γ: 90°
• Cell volume: 6161.3 ± 0.6 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1212
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.155
• Weighted residual factors for all reflections included in the refinement: 0.1891
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No