Crystallography Open Database

Information card for entry 7132965

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Coordinates	7132965.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H33 N O2
Calculated formula	C34 H33 N O2
Title of publication	A two carbon homologation of Friedel-Crafts alkylation enabled by photochemical alkene stitching: modular assembly of cyclolignans.
Authors of publication	Pramanik, Shyamal; Samanta, Apurba; Maity, Soumitra
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	40
Pages of publication	5282 - 5285
a	21.901 ± 0.0016 Å
b	11.9356 ± 0.0011 Å
c	10.1958 ± 0.0008 Å
α	90°
β	95.864 ± 0.007°
γ	90°
Cell volume	2651.3 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1098
Residual factor for significantly intense reflections	0.0544
Weighted residual factors for significantly intense reflections	0.1299
Weighted residual factors for all reflections included in the refinement	0.1538
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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