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Information card for entry 7133005
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Coordinates | 7133005.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H22 N2 O |
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Calculated formula | C23 H22 N2 O |
Title of publication | Facile access to <i>C</i>-substituted piperazin-2-ones and mianserin derivative enabled by chemoselective carbene insertion and cyclization cascade. |
Authors of publication | Kumar, Dharmendra; Unnikrishnan, Urmila; Kuram, Malleswara Rao |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 44 |
Pages of publication | 5691 - 5694 |
a | 10.0123 ± 0.0006 Å |
b | 18.3467 ± 0.0008 Å |
c | 10.107 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1856.58 ± 0.16 Å3 |
Cell temperature | 295 ± 0.1 K |
Ambient diffraction temperature | 295 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 29 |
Hermann-Mauguin space group symbol | P c a 21 |
Hall space group symbol | P 2c -2ac |
Residual factor for all reflections | 0.0402 |
Residual factor for significantly intense reflections | 0.0359 |
Weighted residual factors for significantly intense reflections | 0.0923 |
Weighted residual factors for all reflections included in the refinement | 0.0956 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7133005.html
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