Crystallography Open Database

Information card for entry 7133027

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Coordinates	7133027.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H75 B N4 O2 Si
Calculated formula	C69 H75 B N4 O2 Si
Title of publication	Synthetic, structural and reactivity studies of a boryl-ethynyl Silylene.
Authors of publication	Chen, Wenhao; Hu, Haisheng; Feng, Jie; Zhu, Lei; Wu, Di
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	45
Pages of publication	5828 - 5831
a	11.765 ± 0.0003 Å
b	23.8074 ± 0.0005 Å
c	23.7692 ± 0.0006 Å
α	90°
β	97.721 ± 0.001°
γ	90°
Cell volume	6597.3 ± 0.3 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0573
Residual factor for significantly intense reflections	0.0443
Weighted residual factors for significantly intense reflections	0.1072
Weighted residual factors for all reflections included in the refinement	0.1158
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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