Information card for entry 7133149

Structure parameters

• Formula: C79 H64 B F24 N2 O3 P
• Calculated formula: C79 H64 B F24 N2 O3 P
• Title of publication: P(V)-bis(amidophenolate) ligand cooperation: Stoichiometric C=O-bond cleavage in aldehydes and ketones
• Authors of publication: Karnbrock, Simon Bernhard Hugo; Golz, Christopher; Alcarazo, Manuel
• Journal of publication: Chemical Communications
• Year of publication: 2024
• a: 12.366 ± 0.0008 Å
• b: 20.9073 ± 0.0015 Å
• c: 29.743 ± 0.002 Å
• α: 90°
• β: 97.228 ± 0.002°
• γ: 90°
• Cell volume: 7628.6 ± 0.9 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No