Information card for entry 7133155
| Formula |
C51 H39 Cl2 N O13 |
| Calculated formula |
C51 H39 Cl2 N O13 |
| Title of publication |
Total synthesis of 1,4a-di-<i>epi-ent</i>-pancratistatin, exemplifying a stereodivergent approach to pancratistatin isomers. |
| Authors of publication |
Sun, Chunzhao; Inokuma, Tsubasa; Tsuji, Daisuke; Yamaoka, Yousuke; Akagi, Reiko; Yamada, Ken-Ichi |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2024 |
| Journal volume |
60 |
| Journal issue |
53 |
| Pages of publication |
6757 - 6760 |
| a |
10.8258 ± 0.0001 Å |
| b |
13.1828 ± 0.0002 Å |
| c |
15.3126 ± 0.0002 Å |
| α |
90° |
| β |
79.363 ± 0.001° |
| γ |
90° |
| Cell volume |
2147.78 ± 0.05 Å3 |
| Cell temperature |
93 K |
| Ambient diffraction temperature |
93 K |
| Number of distinct elements |
5 |
| Space group number |
4 |
| Hermann-Mauguin space group symbol |
P 1 21 1 |
| Hall space group symbol |
P 2yb |
| Residual factor for all reflections |
0.0849 |
| Residual factor for significantly intense reflections |
0.0816 |
| Weighted residual factors for significantly intense reflections |
0.2214 |
| Weighted residual factors for all reflections included in the refinement |
0.2299 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.063 |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7133155.html
