Information card for entry 7133171

Structure parameters

• Formula: C38 H53 Au N4 Si
• Calculated formula: C38 H53 Au N4 Si
• Title of publication: Gold(I)-catalyzed homologation of aryl aldehydes with trimethylsilyldiazomethane.
• Authors of publication: Bakhoda, Abolghasem 'Gus'
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 54
• Pages of publication: 6937 - 6940
• a: 13.0228 ± 0.0018 Å
• b: 16.875 ± 0.003 Å
• c: 18.996 ± 0.002 Å
• α: 76.362 ± 0.005°
• β: 79.196 ± 0.005°
• γ: 70.713 ± 0.004°
• Cell volume: 3801.7 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.021
• Residual factor for significantly intense reflections: 0.0172
• Weighted residual factors for significantly intense reflections: 0.0372
• Weighted residual factors for all reflections included in the refinement: 0.0384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No