Information card for entry 7133192

Structure parameters

• Formula: C5 H6 O4
• Calculated formula: C5 H6 O4
• Title of publication: Efficient carbene transfer reactivity mediated by Fe(II) complexes supported by bulky alkoxides.
• Authors of publication: Kulathungage, Lakshani W.; Kurup, Sudheer S.; Browne, Edison A.; Spalink, Gabriel H.; Ward, Cassandra L.; Lord, Richard L.; Groysman, Stanislav
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 55
• Pages of publication: 7033 - 7036
• a: 5.006 ± 0.0004 Å
• b: 7.2628 ± 0.0008 Å
• c: 8.6451 ± 0.0008 Å
• α: 106.71 ± 0.004°
• β: 102.405 ± 0.003°
• γ: 92.116 ± 0.003°
• Cell volume: 292.37 ± 0.05 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110.15 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0616
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for significantly intense reflections: 0.0996
• Weighted residual factors for all reflections included in the refinement: 0.1077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No