Information card for entry 7133198

Structure parameters

• Formula: C29.6 H25.2 Cl1.2 N O3 P
• Calculated formula: C29.6 H25.2 Cl1.2 N O3 P
• Title of publication: Silver-catalyzed P-centered anion nucleophilic addition to isocyanide: Access to 2-phosphinoyl indoles/indol-3-ols
• Authors of publication: Liu, Yong; Jia, Mengying; Wang, Guodong; Yang, Wenhui; Xu, Xianxiu
• Journal of publication: Chemical Communications
• Year of publication: 2024
• a: 9.9338 ± 0.0007 Å
• b: 11.4115 ± 0.0006 Å
• c: 13.4261 ± 0.0009 Å
• α: 91.104 ± 0.005°
• β: 99.247 ± 0.006°
• γ: 107.898 ± 0.005°
• Cell volume: 1425.68 ± 0.17 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0815
• Residual factor for significantly intense reflections: 0.0677
• Weighted residual factors for significantly intense reflections: 0.1921
• Weighted residual factors for all reflections included in the refinement: 0.2079
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No