Information card for entry 7133310

Structure parameters

• Formula: C29 H62 N3 Si3
• Calculated formula: C29 H62 N3 Si3
• Title of publication: A neutral crystalline imino-substituted silyl radical.
• Authors of publication: Kiefer, Fiona J.; Kostenko, Arseni; Holzner, Richard; Inoue, Shigeyoshi
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 65
• Pages of publication: 8577 - 8580
• a: 11.5884 ± 0.001 Å
• b: 17.221 ± 0.0016 Å
• c: 18.536 ± 0.0017 Å
• α: 69.558 ± 0.003°
• β: 80.011 ± 0.003°
• γ: 82.655 ± 0.003°
• Cell volume: 3404.5 ± 0.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0443
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.095
• Weighted residual factors for all reflections included in the refinement: 0.0996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.138
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No