Crystallography Open Database

Information card for entry 7133316

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Coordinates	7133316.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H37 Au F5 P S Si3
Calculated formula	C34 H37 Au F5 P S Si3
Title of publication	Metal-catalyzed valence isomerization of a methylene(thioxo)phosphorane to a thiaphosphirane.
Authors of publication	Ishida, Shintaro; Yoshida, Yusuke; Iwamoto, Takeaki
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	63
Pages of publication	8288 - 8291
a	13.8756 ± 0.0001 Å
b	20.1815 ± 0.0001 Å
c	25.941 ± 0.0002 Å
α	88.525 ± 0.001°
β	87.728 ± 0.001°
γ	75.68 ± 0.001°
Cell volume	7032.08 ± 0.09 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0431
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0549
Weighted residual factors for all reflections included in the refinement	0.0576
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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